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. 2024 Mar 16;9(12):14442–14454. doi: 10.1021/acsomega.4c00112

Table 1. Factorial Design with the Observed Results for the EO Yield and d-Limonene Concentration.

HD time (min) water-to-solid ratio (v/w) EO yield (%) d-limonene concentration (%)
120 4 0.29 37.43
120 5.5 0.35 19.19
120 7 0.38 24.68
180 4 0.45 23.84
180 5.5 0.38 20.49
180 7 0.26 21.21
240 4 0.57 13.37
240 5.5 0.44 18.30
240 7 0.48 14.90
120 4 0.32 14.74
120 5.5 0.29 28.83
120 7 0.78 20.53
180 4 0.23 22.27
180 5.5 0.45 20.83
180 7 0.29 23.92
240 4 0.23 16.60
240 5.5 0.73 21.73
240 7 0.47 20.31