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(A) Change in the UV–vis spectrum of 3 (0.2 mM) upon addition of 1 equiv of (4-OMe-C6H4)3C• to an 1:4 acetonitrile/toluene solution (v/v) of 3 at −60 °C. (B) Plot of 1/[3] vs time for the determination of k2 value for the OH rebound reaction.
