Figure - PMC

Skip to main content

An official website of the United States government

Here's how you know

Here's how you know

Official websites use .gov
A .gov website belongs to an official government organization in the United States.

Secure .gov websites use HTTPS
A lock ( ) or https:// means you've safely connected to the .gov website. Share sensitive information only on official, secure websites.

View full-text article in PMC

. 2024 Mar 30;15:2777. doi: 10.1038/s41467-024-47071-4

Search in PMC
Search in PubMed
View in NLM Catalog
Add to search

© The Author(s) 2024

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/.

PMC Copyright notice

Fig. 3 — a Schematic and b real instrument for the operando ambient pressure experiment. c XPS spectra of the LLZO pellet before and after vacuum annealing at room temperature. d The influence of temperature rise on the ratios of O(lattice)/O(CO₃^2-) and C(CO₃^2-)/C(C-C). e In situ mass spectrum results in the temperature range of 160 – 370 °C. CO₂ and H₂O are simultaneously observed to be the decomposition products at around 300 °C. f The schematic illustration of reaction of xLi₂CO₃ + Li_6.5-2xH_2xLa₃Zr_1.5Ta_0.5O₁₂ → Li_6.5La₃Zr_1.5Ta_0.5O₁₂ + xH₂O + xCO₂ at the LLZO surface during the vacuum annealing process.