Table 2. Precision of SB-PS-MS Analysis: Intra-Day Analysis was Conducted with Three Triplicates Measured on Three Different Days.
| AA | intra-day |
||
|---|---|---|---|
| day 1 | day 2 | day 3 | |
| RSD (%) | RSD (%) | RSD (%) | |
| Gly | 4.4 | 5.0 | 0.6 |
| Ala | 2.7 | 3.5 | 1.4 |
| Ser | 15 | 15 | 1.0 |
| Pro | 2.8 | 3.3 | 1.6 |
| Val | 2.0 | 1.8 | 0.9 |
| Thr | 14 | 6.7 | 1.8 |
| Leu + Ile | 3.9 | 12 | 0.9 |
| Asp | 16 | 9.5 | 12 |
| Lys | 27 | 37 | 12 |
| Glu | 59 | 69 | 25 |
| Met | 16 | 36 | 9.5 |
| His | 38 | 38 | 23 |
| Phe | 3.8 | 1.2 | 5.9 |
| Arg | 13 | 11 | 6.9 |
| Tyr | 11 | 2.0 | 9.1 |