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. 2024 Mar 20;96(13):5289–5297. doi: 10.1021/acs.analchem.4c00215

Table 2. Precision of SB-PS-MS Analysis: Intra-Day Analysis was Conducted with Three Triplicates Measured on Three Different Days.

AA intra-day
  day 1 day 2 day 3
  RSD (%) RSD (%) RSD (%)
Gly 4.4 5.0 0.6
Ala 2.7 3.5 1.4
Ser 15 15 1.0
Pro 2.8 3.3 1.6
Val 2.0 1.8 0.9
Thr 14 6.7 1.8
Leu + Ile 3.9 12 0.9
Asp 16 9.5 12
Lys 27 37 12
Glu 59 69 25
Met 16 36 9.5
His 38 38 23
Phe 3.8 1.2 5.9
Arg 13 11 6.9
Tyr 11 2.0 9.1