| Crystal data |
| Chemical formula |
[Ru(C19H13N5)2](PF6)2·3C4H10O |
|
M
r
|
1236.05 |
| Crystal system, space group |
Orthorhombic, P
c
a21
|
| Temperature (K) |
125 |
|
a, b, c (Å) |
26.718 (4), 9.8834 (13), 20.648 (3) |
|
V (Å3) |
5452.4 (12) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.44 |
| Crystal size (mm) |
0.26 × 0.18 × 0.12 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.027, 0.049 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
54516, 11121, 9404 |
|
R
int
|
0.058 |
| (sin θ/λ)max (Å−1) |
0.625 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.092, 0.199, 1.18 |
| No. of reflections |
11121 |
| No. of parameters |
716 |
| No. of restraints |
1049 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
2.08, −1.44 |
| Absolute structure |
Refined as an inversion twin |
| Absolute structure parameter |
0.45 (12) |
