| Stoe IPDS 2 diffractometer | 1314 reflections with I > 2σ(I) |
| Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus, Incoatec Iµs | Rint = 0.027 |
| Plane graphite monochromator | θmax = 26.1°, θmin = 2.5° |
| Detector resolution: 6.67 pixels mm-1 | h = −10→10 |
| rotation method scans | k = −5→5 |
| 4973 measured reflections | l = −27→27 |
| 1735 independent reflections |
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