| Bruker D8 QUEST PHOTON 3 diffractometer | 7105 independent reflections |
| Radiation source: fine-focus sealed tube | 6502 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.052 |
| Detector resolution: 7.3910 pixels mm-1 | θmax = 33.2°, θmin = 2.8° |
| φ and ω scans | h = −13→13 |
| Absorption correction: numerical (SADABS; Krause et al., 2015) | k = −22→22 |
| Tmin = 0.98, Tmax = 0.98 | l = −23→23 |
| 142315 measured reflections |