| Bruker D8 VENTURE PHOTON 3 CPAD diffractometer | 2495 independent reflections |
| Radiation source: INCOATEC IµS micro–focus source | 2468 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.050 |
| Detector resolution: 7.3910 pixels mm-1 | θmax = 72.6°, θmin = 3.9° |
| φ and ω scans | h = −28→28 |
| Absorption correction: multi-scan (SADABS; Krause et al., 2015) | k = −5→5 |
| Tmin = 0.60, Tmax = 0.72 | l = −14→14 |
| 22953 measured reflections |