| Crystal data |
| Chemical formula |
C17H12N2O |
|
M
r
|
260.29 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
120 |
|
a, b, c (Å) |
8.4614 (14), 9.0947 (15), 9.5360 (16) |
| α, β, γ (°) |
87.739 (2), 72.963 (2), 69.028 (2) |
|
V (Å3) |
653.39 (19) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.08 |
| Crystal size (mm) |
0.34 × 0.33 × 0.14 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEX CCD |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.91, 0.99 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
12629, 3456, 2869 |
|
R
int
|
0.026 |
| (sin θ/λ)max (Å−1) |
0.684 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.044, 0.139, 1.17 |
| No. of reflections |
3456 |
| No. of parameters |
181 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.42, −0.24 |
