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. 2024 Apr 1;16(7):1031. doi: 10.3390/nu16071031

Table 1.

The gradient program for the chromatographic method.

Time % A % B
Conditions 0 10 90
3 12 88
6 14 86
9 16 84
12 18 82
32 26 74
40 36 64
50 50 50
55 100 0
57 10 90
60 10 90