Skip to main content
. 2024 Apr 16;14(17):12147–12157. doi: 10.1039/d4ra01483a
No. 5 6 7
δ C δ H (mult., J in Hz) δ C δ H (mult., J in Hz) δ C δ H (mult., J in Hz)
1 39.8 0.99 (m)/1.63 (m) 39.8 0.98 (m)/1.64 (m) 39.78 0.98 (m)/1.64 (m)
2 27.0 1.72 (m)/1.87 (m) 27.0 1.72 (m)/1.86 (m) 27.0 1.70 (m)/1.87 (m)
3 90.7 3.15 (dd, 11.4, 4.2) 90.7 3.16 (dd, 11.4, 4.2) 90.7 3.15 (dd, 11.4, 4.2)
4 40.7 40.8 40.8
5 57.1 0.80 (br d, 11.4) 57.1 0.80 (br d, 11.4) 57.1 0.80 (br d, 11.4)
6 19.4 1.43 (m)/1.56 (m) 19.4 1.43 (m)/1.56 (m) 19.4 1.42 (m)/1.55 (m)
7 33.9 1.33 (m)/1.52 (m) 33.9 1.33 (m)/1.52 (m) 34.0 1.33 (m)/1.50 (m)
8 40.1 40.2 40.2
9 49.0 1.60 (m) 49.0 1.60 (m) 49.0 1.59 (m)
10 37.9 38.0 37.9
11 24.6 1.92–1.94 (m) 24.6 1.90–1.92 (m) 24.6 1.90–1.93 (m)
12 124.0 5.31 (t, 3.6) 123.8 5.34 (t, 3.0) 123.9 5.29 (t, 3.0)
13 144.6 144.6 144.8
14 42.9 42.9 42.9
15 28.9 1.10 (m)/1.78 (m) 28.9 1.10 (m)/1.80 (m) 28.9 1.10 (m)/1.80 (m)
16 24.3 1.76 (m)/2.10 (td, 13.2, 3.0) 23.8 1.74 (m)/2.04 (td, 13.2, 3.0) 24.1 1.73 (m)/2.07 (td, 13.8, 2.4)
17 49.0 47.7 48.4
18 41.9 2.85 (dd, 13.2, 4.2) 41.5 3.09 (dd, 13.8, 4.2) 41.8 2.91 (dd, 13.8, 4.2)
19 42.5 1.40a/1.62a 46.1 1.47a 1.84 (t, 13.8) 41.4 1.11a 1.83 (t, 13.8)
20 36.1 69.8 36.8
21 29.9 1.31 (m)/1.52 (m) 34.1 1.50 (m)/1.56 (m) 29.3 1.19 (m)/1.50 (m)
22 32.8 1.58 (m)/1.72 (m) 32.5 1.57 (m)/1.94 (m) 32.5 1.66 (m)/1.74 (m)
23 28.6 1.06 (s) 28.6 1.06 (s) 28.6 1.06 (s)
24 17.0 0.87 (s) 17.0 0.88 (s) 17.0 0.87 (s)
25 16.1 0.98 (s) 16.2 0.98 (s) 16.1 0.98 (s)
26 17.9 0.82 (s) 18.0 0.84 (s) 17.9 0.83 (s)
27 26.3 1.19 (s) 26.3 1.17 (s) 26.3 1.19 (s)
28 178.1 178.0 178.0
29 28.0 0.92 (s) 31.5 1.20 (s) 74.3 3.21 (s)
30 66.3 3.45a/3.54a 19.6 0.95 (s)
a

Overlapped signal.