No. | 5 | 6 | 7 | |||
---|---|---|---|---|---|---|
δ C | δ H (mult., J in Hz) | δ C | δ H (mult., J in Hz) | δ C | δ H (mult., J in Hz) | |
1 | 39.8 | 0.99 (m)/1.63 (m) | 39.8 | 0.98 (m)/1.64 (m) | 39.78 | 0.98 (m)/1.64 (m) |
2 | 27.0 | 1.72 (m)/1.87 (m) | 27.0 | 1.72 (m)/1.86 (m) | 27.0 | 1.70 (m)/1.87 (m) |
3 | 90.7 | 3.15 (dd, 11.4, 4.2) | 90.7 | 3.16 (dd, 11.4, 4.2) | 90.7 | 3.15 (dd, 11.4, 4.2) |
4 | 40.7 | — | 40.8 | — | 40.8 | — |
5 | 57.1 | 0.80 (br d, 11.4) | 57.1 | 0.80 (br d, 11.4) | 57.1 | 0.80 (br d, 11.4) |
6 | 19.4 | 1.43 (m)/1.56 (m) | 19.4 | 1.43 (m)/1.56 (m) | 19.4 | 1.42 (m)/1.55 (m) |
7 | 33.9 | 1.33 (m)/1.52 (m) | 33.9 | 1.33 (m)/1.52 (m) | 34.0 | 1.33 (m)/1.50 (m) |
8 | 40.1 | — | 40.2 | — | 40.2 | — |
9 | 49.0 | 1.60 (m) | 49.0 | 1.60 (m) | 49.0 | 1.59 (m) |
10 | 37.9 | — | 38.0 | — | 37.9 | — |
11 | 24.6 | 1.92–1.94 (m) | 24.6 | 1.90–1.92 (m) | 24.6 | 1.90–1.93 (m) |
12 | 124.0 | 5.31 (t, 3.6) | 123.8 | 5.34 (t, 3.0) | 123.9 | 5.29 (t, 3.0) |
13 | 144.6 | — | 144.6 | — | 144.8 | — |
14 | 42.9 | — | 42.9 | — | 42.9 | — |
15 | 28.9 | 1.10 (m)/1.78 (m) | 28.9 | 1.10 (m)/1.80 (m) | 28.9 | 1.10 (m)/1.80 (m) |
16 | 24.3 | 1.76 (m)/2.10 (td, 13.2, 3.0) | 23.8 | 1.74 (m)/2.04 (td, 13.2, 3.0) | 24.1 | 1.73 (m)/2.07 (td, 13.8, 2.4) |
17 | 49.0 | — | 47.7 | — | 48.4 | — |
18 | 41.9 | 2.85 (dd, 13.2, 4.2) | 41.5 | 3.09 (dd, 13.8, 4.2) | 41.8 | 2.91 (dd, 13.8, 4.2) |
19 | 42.5 | 1.40a/1.62a | 46.1 | 1.47a 1.84 (t, 13.8) | 41.4 | 1.11a 1.83 (t, 13.8) |
20 | 36.1 | — | 69.8 | — | 36.8 | — |
21 | 29.9 | 1.31 (m)/1.52 (m) | 34.1 | 1.50 (m)/1.56 (m) | 29.3 | 1.19 (m)/1.50 (m) |
22 | 32.8 | 1.58 (m)/1.72 (m) | 32.5 | 1.57 (m)/1.94 (m) | 32.5 | 1.66 (m)/1.74 (m) |
23 | 28.6 | 1.06 (s) | 28.6 | 1.06 (s) | 28.6 | 1.06 (s) |
24 | 17.0 | 0.87 (s) | 17.0 | 0.88 (s) | 17.0 | 0.87 (s) |
25 | 16.1 | 0.98 (s) | 16.2 | 0.98 (s) | 16.1 | 0.98 (s) |
26 | 17.9 | 0.82 (s) | 18.0 | 0.84 (s) | 17.9 | 0.83 (s) |
27 | 26.3 | 1.19 (s) | 26.3 | 1.17 (s) | 26.3 | 1.19 (s) |
28 | 178.1 | — | 178.0 | — | 178.0 | — |
29 | 28.0 | 0.92 (s) | 31.5 | 1.20 (s) | 74.3 | 3.21 (s) |
30 | 66.3 | 3.45a/3.54a | — | — | 19.6 | 0.95 (s) |
Overlapped signal.