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. 2024 Apr 8;12:102693. doi: 10.1016/j.mex.2024.102693

Table 3.

GC and MSD conditions for the analysis of OPEs and IS.

Analyte Retention Time (min) SIM Acquisition Window (min) Quantitation Ion, m/z Confirmation Ion(s), m/z Ion Dwell Time (ms)
HMB (IS) 7.8 6.00 – 9.50 147.1 117.0 40
TCPP 9.1 6.00 – 9.50 277.0 201.0
279.0
40
TDCPP 10.9 9.50 – 11.00 381.0 191.0
209.0
383.0
50
TPHP 11.1 11.00 – 12.00 326.0 215.0
233.0
325.0
50
T24DtBPP 19.1 12.00 – 24.17 647.5 648.4
662.5
663.4
80