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. 2024 Apr 22;14:9181. doi: 10.1038/s41598-024-58845-7

Table 1.

The synthesis of (9R)-HHC and (9S)-HHC at different scales.

Entry Synthesis scale (∆8-THC mass), g Mass of 5% Pd/C per 1 g of ∆8-THC, mg 8-THC concentration, g/L Duration of the reduction, days 9R:9S molar ratio
1 10 50 200 2 3:1
2 10 20 50 2 3:2
3 250 50 200 5 3:1
4 1000 50 250 14 3:1