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. 2024 May 1;11(Pt 3):299–308. doi: 10.1107/S2052252524001969

Table 2. SAXS data collection statistics.

Data collection parameters
Instrument SAXS/WAXS beamline at the Australian Synchrotron
Detector Pilatus 1M
Beam geometry point
Wavelength (Å) 1.0332
Camera length (mm) 3252
q range (Å−1) 0.005-0.292
Exposure time (s) 1
Concentration range (mg ml−1) 0.15–2.4
Temperature (K) 285
 
Structural parameters†
I(0) (cm−1) [from P(r)] 0.48
R g (Å) [from P(r)] 43.99
I(0) (cm−1) [from Guinier] 0.48
R g (Å) [from Guinier] 43.85
D max (Å) 153.06
Calculated molecular mass‡ [from I(0)] (kDa) 276.9
Calculated molecular mass (from SAXS MoW2) (kDa) 269.0
Molecular mass from sequence (kDa) 273.8
 
Software employed
Primary data reduction scatterBrain
Data processing PRIMUS
Ab initio analysis DAMMIF/DAMMIN
Validation and averaging DAMAVER
Computation of model intensities CRYSOL §
Three-dimensional graphics representation PyMOL
†

Calculated for a 2.4 mg ml−1 concentration.

‡

Calculated from data placed on an absolute scale and using a partial specific volume of 0.7425 cm3 g−1.

§

Svergun et al. (1995 ▸).