Table 2. SAXS data collection statistics.
| Data collection parameters | |
| Instrument | SAXS/WAXS beamline at the Australian Synchrotron |
| Detector | Pilatus 1M |
| Beam geometry | point |
| Wavelength (Å) | 1.0332 |
| Camera length (mm) | 3252 |
| q range (Å−1) | 0.005-0.292 |
| Exposure time (s) | 1 |
| Concentration range (mg ml−1) | 0.15–2.4 |
| Temperature (K) | 285 |
| Structural parameters† | |
| I(0) (cm−1) [from P(r)] | 0.48 |
| R g (Å) [from P(r)] | 43.99 |
| I(0) (cm−1) [from Guinier] | 0.48 |
| R g (Å) [from Guinier] | 43.85 |
| D max (Å) | 153.06 |
| Calculated molecular mass‡ [from I(0)] (kDa) | 276.9 |
| Calculated molecular mass (from SAXS MoW2) (kDa) | 269.0 |
| Molecular mass from sequence (kDa) | 273.8 |
| Software employed | |
| Primary data reduction | scatterBrain |
| Data processing | PRIMUS |
| Ab initio analysis | DAMMIF/DAMMIN |
| Validation and averaging | DAMAVER |
| Computation of model intensities | CRYSOL § |
| Three-dimensional graphics representation | PyMOL |
Calculated for a 2.4 mg ml−1 concentration.
Calculated from data placed on an absolute scale and using a partial specific volume of 0.7425 cm3 g−1.
Svergun et al. (1995 ▸).