| Crystal data |
| Chemical formula |
C15H22O |
|
M
r
|
218.34 |
| Crystal system, space group |
Monoclinic, C2/c
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
25.6112 (6), 9.7565 (2), 10.3664 (2) |
| β (°) |
95.169 (2) |
|
V (Å3) |
2579.78 (10) |
|
Z
|
8 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
0.52 |
| Crystal size (mm) |
0.35 × 0.10 × 0.01 |
| |
| Data collection |
| Diffractometer |
XtaLAB Synergy R, DW system, HyPix-Arc 150 |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku OD, 2023 ▸) |
|
T
min, T
max
|
0.601, 1.000 |
| No. of measured, independent and observed [I ≥ 2u(I)] reflections |
13789, 2579, 2244 |
|
R
int
|
0.026 |
| (sin θ/λ)max (Å−1) |
0.624 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.029, 0.077, 1.07 |
| No. of reflections |
2579 |
| No. of parameters |
343 |
| H-atom treatment |
All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) |
0.15, −0.19 |
