| Xcalibur, Eos, Gemini diffractometer | 3950 independent reflections |
| Radiation source: fine-focus sealed X-ray tube, Enhance (Cu) X-ray Source | 3693 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.050 |
| Detector resolution: 16.2312 pixels mm-1 | θmax = 70.5°, θmin = 3.4° |
| ω scans | h = −31→31 |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2023) | k = −8→6 |
| Tmin = 0.419, Tmax = 1.000 | l = −16→16 |
| 20069 measured reflections |
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