Oxford Diffraction Xcalibur, Eos diffractometer | 1864 independent reflections |
Radiation source: fine-focus sealed X-ray tube | 1581 reflections with I > 2σ(I) |
Detector resolution: 16.1419 pixels mm-1 | Rint = 0.070 |
ω scan | θmax = 31.1°, θmin = 2.4° |
Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2015) | h = −14→14 |
Tmin = 0.240, Tmax = 1.000 | k = −10→10 |
28605 measured reflections | l = −22→22 |