Refinement on F2
|
Secondary atom site location: difference Fourier map |
Least-squares matrix: full |
Hydrogen site location: mixed |
R[F2 > 2σ(F2)] = 0.030 |
H atoms treated by a mixture of independent and constrained refinement |
wR(F2) = 0.050 |
w = 1/[σ2(Fo2) + (0.0121P)2 + 3.4353P] where P = (Fo2 + 2Fc2)/3 |
S = 1.11 |
(Δ/σ)max < 0.001 |
1864 reflections |
Δρmax = 1.56 e Å−3
|
65 parameters |
Δρmin = −1.18 e Å−3
|
0 restraints |
Extinction correction: SHELXL2019/3 (Sheldrick, 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
|
Primary atom site location: structure-invariant direct methods |
Extinction coefficient: 0.00051 (4) |