Oxford Diffraction Xcalibur, Eos diffractometer | 2887 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 2134 reflections with I > 2σ(I) |
Detector resolution: 16.1419 pixels mm-1 | Rint = 0.080 |
ω scan | θmax = 29.1°, θmin = 2.6° |
Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2015) | h = −17→17 |
Tmin = 0.702, Tmax = 1.000 | k = −11→11 |
53277 measured reflections | l = −27→27 |