Oxford Diffraction Xcalibur, Eos diffractometer | 3371 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 2495 reflections with I > 2σ(I) |
Detector resolution: 16.1419 pixels mm-1 | Rint = 0.074 |
ω scan | θmax = 30.0°, θmin = 2.5° |
Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2015) | h = −17→17 |
Tmin = 0.380, Tmax = 1.000 | k = −11→12 |
38297 measured reflections | l = −29→29 |