Table 2.
13C NMR spectral data of compounds 1, 2, and 4–6 (100 MHz in CDCl3).
| No. | 1 | 2 | 4 | 5 | 6 |
|---|---|---|---|---|---|
| 1 | 35.2 | 40.0 | 39.6 | 40.8 | 38.1 |
| 2 | 18.7 | 19.0 | 18.9 | 17.9 | 18.1 |
| 3 | 40.5 | 41.5 | 41.6 | 38.4 | 41.0 |
| 4 | 37.2 | 35.0 | 35.7 | 37.4 | 37.0 |
| 5 | 91.6 | 61.4 | 67.6 | 96.0 | 96.3, |
| 6 | 105.1 | 73.4 | 36.6 | 47.0 | |
| 7 | 164.6 | 170.1 | 171.1 | 172.4 | 200.8 |
| 8 | 118.4 | 124.2 | 143.7 | 147.3 | 149.7 |
| 9 | 144.3 | 148.9 | 137.3 | 136.8 | 136.4 |
| 10 | 37.1 | 39.8 | 38.4 | 48.6 | 47.9 |
| 11 | 109.0 | 110.4 | 111.4 | 109.2 | 108.6 |
| 12 | 157.4 | 155.7 | 149.4 | 147.7 | 147.0 |
| 13 | 132.7 | 131.6 | 133.9 | 133.7 | 134.0 |
| 14 | 129.0 | 130.0 | 117.9 | 107.9 | 107.3 |
| 15 | 27.2 | 27.1 | 27.2 | 27.6 | 27.4 |
| 16 | 22.7 | 22.8 | 22.5 | 22.9 | 23.1 |
| 17 | 22.7 | 22.7 | 22.7 | 23.0 | 23.0 |
| 18 | 22.0 | 32.8 | 32.6 | 28.5 | 28.1 |
| 19 | 30.9 | 22.6 | 22.6 | 26.0 | 25.6 |
| 20 | 34.0 | 22.8 | 20.3 | 19.9 | 19.5 |
| 6-OCH3 | 56.5 |