表4.

鸡蛋、鹅蛋和鸭蛋样品中31种兽药的平均回收率和相对标准偏差(n=6)

Drug	Spiked/ (μg/kg)	Egg			Goose egg			Duck egg
		Recovery/%	RSD/%		Recovery/%	RSD/%		Recovery/%	RSD/%
Levamisole	2	90.1	8.0		92.3	7.3		83.2	8.9
	5	81.8	10.2		85.3	6.4		88.0	7.3
	10	98.3	4.2		95.2	7.0		91.2	10.0
Trimethoprim	3	75.5	2.0		82.3	3.4		73.4	6.3
	10	78.5	1.8		90.2	7.6		84.2	5.5
	20	93.5	5.9		84.3	5.1		78.1	4.8
Tilmicosin	3	81.6	13.8		78.3	10.9		80.4	11.1
	10	93.6	15.2		85.4	7.5		86.8	9.1
	20	95.2	11.9		90.1	9.4		92.0	10.3
Danofloxacin	3	80.7	15.0		83.5	8.9		81.3	7.4
	10	84.7	6.1		76.7	11.2		77.8	6.6
	20	85.9	4.1		80.6	7.2		90.3	3.8
Enrofloxacin	3	73.5	11.3		70.7	10.6		69.3	9.8
	10	77.9	7.9		80.6	8.5		75.9	6.3
	20	81.6	2.8		78.2	6.7		82.3	8.0
Ciprofloxacin	3	69.4	12.3		72.3	8.9		68.5	11.8
	10	76.1	8.3		80.2	10.2		75.4	9.8
	20	82.0	5.5		78.9	7.7		83.7	5.6
Flumequine	3	83.3	7.2		90.5	8.4		87.4	9.4
	10	92.9	7.9		86.7	5.1		84.3	6.5
	20	102.3	3.8		95.6	6.3		96.0	5.8
Oxolinic acid	3	92.3	14.2		88.6	9.3		89.1	12.3
	10	86.9	8.7		96.3	11.5		86.7	8.9
	20	94.2	5.4		94.0	8.4		84.0	9.7
Sarafloxacin	3	71.7	15.2		67.5	13.3		66.2	16.4
	5	73.3	7.9		72.3	9.4		70.8	13.2
	10	81.6	3.2		78.2	6.8		74.3	8.9
Lomefloxacin	2	71.0	9.4		70.4	8.5		68.3	9.6
	4	75.3	11.9		69.8	6.8		73.6	7.3
	8	79.7	6.5		78.6	5.3		81.0	8.4
Norfloxacin	1	73.2	5.6		68.5	8.5		65.7	11.0
	2	78.1	3.4		73.8	4.8		68.4	7.6
	4	83.5	4.8		79.1	6.4		75.5	4.8
Ofloxacin	1	79.7	6.9		80.3	5.8		76.7	7.8
	2	85.3	5.0		84.5	3.3		80.6	5.0
	4	90.4	3.2		91.6	4.1		87.6	6.1
Pefloxacin	2	79.7	14.5		70.3	15.8		61.2	9.4
	4	79.8	12.8		74.9	10.4		70.5	8.7
	8	86.4	12.1		81.7	8.8		78.9	10.2
Doxycycline	10	69.2	14.7		70.3	12.3		66.8	13.4
	20	67.2	10.3		68.4	9.2		72.3	11.6
	40	73.5	6.3		75.9	10.5		74.0	8.7
Sulfadimidine	3	91.7	5.6		88.6	11.3		85.7	8.9
	10	86.8	11.9		97.5	8.7		90.6	3.4
	20	94.7	10.3		104.5	5.1		97.3	4.0
Sulfadiazine	3	68.7	10.6		68.5	12.3		70.4	10.6
	10	71.4	12.0		74.3	8.9		73.0	8.2
	20	73.9	6.4		81.5	6.0		82.0	7.7
Sulfathiazole	3	71.2	5.9		69.0	12.1		67.4	9.8
	10	76.7	13.9		73.1	8.7		75.0	7.9
	20	76.0	6.4		77.2	5.9		80.4	6.0
Sulfamerazine	3	74.1	16.3		76.5	13.5		72.3	12.3
	10	80.4	12.8		82.4	11.3		78.5	9.9
	20	85.4	9.4		90.1	8.8		85.7	6.8
Sulfameter	3	71.7	10.9		82.3	8.4		78.4	6.5
	10	84.1	13.4		87.6	7.6		80.2	4.5
	20	84.5	8.2		93.5	5.4		88.0	2.1
Sulfamonomethoxine	3	79.5	3.6		80.6	5.6		82.3	6.5
	10	88.1	10.1		90.3	6.0		79.1	4.8
	20	85.7	6.9		102.1	4.4		89.7	3.9
Sulfachloropyridazine	3	77.0	17.6		73.4	12.3		70.9	8.9
	10	78.2	14.7		82.1	8.7		82.3	7.4
	20	84.2	7.0		79.3	6.5		86.4	6.0
Sulfadoxine	3	83.3	8.2		78.3	7.8		83.1	8.2
	10	87.2	12.4		86.0	8.4		86.7	9.1
	20	92.0	5.7		95.5	6.0		92.4	5.5
Sulfadimethoxine	3	87.5	2.7		83.5	6.5		79.6	7.3
	10	86.9	10.5		90.5	4.8		85.4	8.0
	20	90.8	5.0		93.0	3.0		92.4	7.1
Sulfamethoxazole	3	72.3	6.9		70.3	8.4		72.6	6.8
	10	84.3	13.4		77.8	6.3		80.1	7.5
	20	89.0	4.0		86.7	5.0		84.5	6.0
Sulfaquinoxaline	3	61.7	8.2		63.4	10.5		65.0	8.2
	10	66.1	12.2		70.3	8.3		69.4	9.4
	20	75.6	4.1		76.0	5.6		75.7	7.0
Florfenicol-amine	3	85.3	7.4		83.5	6.1		81.0	8.0
	10	88.0	8.2		90.2	3.4		87.3	6.7
	20	90.1	6.1		89.2	4.6		92.2	3.1
Thiamphenicol	1	93.9	10.8		89.4	6.7		90.4	6.5
	10	99.7	10.3		95.0	5.2		93.5	4.7
	20	101.9	2.3		105.7	2.8		96.1	2.5
Florfenicol	1	86.6	11.4		83.4	9.3		85.6	10.3
	10	85.0	4.1		87.2	7.6		90.7	8.7
	20	96.9	1.9		93.5	5.9		91.5	6.2
Toltrazuril sulfone	5	63.4	10.6		65.3	8.6		67.4	9.7
	10	66.4	8.3		72.1	7.8		69.0	10.3
	20	68.5	8.0		74.0	5.5		65.2	7.3
Diclazuril	5	68.4	10.2		70.4	8.3		66.3	10.2
	10	74.3	7.0		68.5	9.9		72.1	8.7
	20	75.0	6.2		74.6	6.8		76.0	7.0
Salicylic acid	3	73.1	11.4		76.4	12.4		80.2	13.5
	10	83.5	3.1		73.1	13.0		82.1	11.7
	20	88.2	4.2		85.3	9.4		89.0	8.7