The d-spacing, SF, texture coefficient, and standard deviation of GDC-00, -10, -20, and -30 ceramics'.
System | h | k | l | 2θ (°) | Intensity | d values (nm) | SF | C i | σ | |||
---|---|---|---|---|---|---|---|---|---|---|---|---|
Reporteda | Observedb | Calculatedc | Calculatedd | |||||||||
GDC-00 | 1 | 1 | 1 | 28.7430 | 100.00 | 0.3124 | 0.3103 | 0.3104 | 0.3104 | 0.001013 | 0.7501 | 0.1566 |
2 | 0 | 0 | 33.2750 | 039.80 | 0.2706 | 0.2690 | 0.2691 | 0.2691 | 0.000865 | 1.1057 | ||
2 | 2 | 0 | 47.6670 | 060.60 | 0.1913 | 0.1906 | 0.1907 | 0.1907 | 0.000805 | 0.9882 | ||
3 | 1 | 1 | 56.5240 | 052.40 | 0.1632 | 0.1627 | 0.1627 | 0.1627 | 0.000730 | 1.1560 | ||
GDC-10 | 1 | 1 | 1 | 28.9820 | 100.00 | 0.3128 | 0.3078 | 0.3079 | 0.3079 | 0.001052 | 0.5658 | 0.4503 |
2 | 0 | 0 | 33.5050 | 086.80 | 0.2709 | 0.2672 | 0.2673 | 0.2673 | 0.001056 | 1.7353 | ||
2 | 2 | 0 | 47.8690 | 059.10 | 0.1916 | 0.1899 | 0.1899 | 0.1899 | 0.000823 | 0.7145 | ||
3 | 1 | 1 | 56.7000 | 060.20 | 0.1634 | 0.1622 | 0.1623 | 0.1623 | 0.000770 | 0.9844 | ||
GDC-20 | 1 | 1 | 1 | 29.3250 | 100.00 | 0.3126 | 0.3043 | 0.3044 | 0.3044 | 0.00111 | 2.3349 | 0.6401 |
2 | 0 | 0 | 33.8530 | 044.60 | 0.2708 | 0.2646 | 0.2646 | 0.2646 | 0.00110 | 0.7498 | ||
2 | 2 | 0 | 48.2070 | 013.40 | 0.1915 | 0.1886 | 0.1887 | 0.1887 | 0.00154 | 0.5928 | ||
3 | 1 | 1 | 57.0100 | 008.40 | 0.1634 | 0.1614 | 0.1615 | 0.1615 | 0.00167 | 0.3225 | ||
GDC-30 | 1 | 1 | 1 | 29.6760 | 089.40 | 0.3135 | 0.3008 | 0.3009 | 0.3009 | 0.00230 | 0.3998 | 0.1246 |
2 | 0 | 0 | 34.2170 | 081.90 | 0.2715 | 0.2618 | 0.2619 | 0.2619 | 0.00177 | 1.2630 | ||
2 | 2 | 0 | 48.5160 | 100.00 | 0.1920 | 0.1875 | 0.1875 | 0.1875 | 0.00128 | 1.0908 | ||
3 | 1 | 1 | 57.2890 | 086.40 | 0.1638 | 0.1607 | 0.1607 | 0.1607 | 0.00120 | 1.2464 |
ICDD card numbers: GDC-00: 00-043-1002, GDC-10: 01-075-0161, GDC-20: 00-050-0201, and GDC-30: 00-046-0507.
XRD pattern of the bulk.
Bragg's law.
Bravais theory.