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. 2024 May 13;14(22):15455–15467. doi: 10.1039/d4ra01902d

Crystallite size and strain values of GDC-00, -10, -20, and -30 ceramicsa.

System Method Scherrer Monshi W–H (UDM) SSP H–W
GDC-00 D (nm) 69.7096 73.2469 72.6126 70.7602 78.7724
ε (×10−3) 0.0394 −0.0170 −0.1641 −1.0646
GDC-10 D (nm) 11.6418 63.9861 60.5633 64.8084 71.9114
ε (×10−3) 0.0075 −0.1734 −0.1809 −1.1738
GDC-20 D (nm) 81.8293 294.8843 185.3047 205.8943
ε (×10−3) 0.6150 2.5 1.4885 9.6591
GDC-30 D (nm) 102.5623 29.6531 24.0781 28.5370 31.7365
ε (×10−3) 0.2352 −1.51 −0.8737 −5.6698
a

Compressive stress, denoted by a negative ε value for GDC, results from the assertion of equal and opposing pressures, which in turn causes the crystalline structure to shrink.32,33