Figure 5.
Influence of base equivalents in the nitrobenzene TH. Reaction conditions: nitrobenzene in EG (0.5 M, 1 eq) and KOH. Flow rate: 0.03 mL/min, 250 mg of CuNPs/Celite 5% w/w, setup B (see Figure S1B). Reaction temperature: 130 °C, and the reaction is monitored after 18 reactor volumes. Reaction yield was determined by GC-MS.