Table 1.
Hydrolysis ratio (h) and temperature (T) of the synthesis; cubic lattice parameters (a); average crystallite size (dXRPD); primary crystals size (dTEM); aggregates size (DTEM). Unities indicated in parentheses.
| Sample | h | T (°C) | a (Å) | dXRPD (nm) | dTEM (nm) | DTEM aggr. (nm) |
|---|---|---|---|---|---|---|
| DEG-b180 | 46 | 180 | 4.268 | 11 | 4 | 104 |
| TTEG-a180 | 7 | 180 | 4.273 | 9 | 7 | 24 |
| TTEG-a205 | 7 | 205 | 4.270 | 12 | 14 | 39 |
| TTEG-a235 | 7 | 235 | 4.268 | 15 | 15 | 44 |
| TTEG-b180 | 46 | 180 | 4.273 | 17 | 8 | 53 |
| TTEG-b205 | 46 | 205 | 4.269 | 18 | 10 | 154 |
| TTEG-b235 | 46 | 235 | 4.267 | 21 | 23 | 111 |
| TTEG1 | 7 | 205 | 4.261 | 7 | 4 | 18 |
| TTEG2 | 46 | 205 | 4.266 | 13 | 4 | 78 |