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. 2024 May 31;9(Pt 5):x240475. doi: 10.1107/S2414314624004759
Br1—C4 1.896 (3) C21—C22 1.388 (5)
N1—C20 1.401 (4) C13—C14 1.353 (5)
N1—C21 1.404 (4) C13—H13 0.9300
N1—H55 0.78 (4) C6—C7 1.352 (5)
C3—C4 1.396 (4) C6—H6 0.9300
C3—C2 1.430 (4) C7—H7 0.9300
C3—C12 1.432 (4) C16—C17 1.383 (5)
C12—C11 1.405 (4) C16—H16 0.9300
C12—C13 1.429 (4) C26—C25 1.385 (5)
C11—C10 1.405 (4) C26—H26 0.9300
C11—C15 1.497 (4) C18—C17 1.366 (5)
C5—C4 1.400 (4) C18—C19 1.375 (5)
C5—C6 1.428 (4) C18—H18 0.9300
C5—C10 1.437 (4) C1—C14 1.392 (5)
C10—C9 1.427 (4) C1—H1 0.9300
C15—C20 1.386 (4) C19—H19 0.9300
C15—C16 1.390 (4) C22—C23 1.371 (5)
C9—C8 1.351 (5) C22—H22 0.9300
C9—H9 0.9300 C17—H17 0.9300
C20—C19 1.395 (4) C14—H14 0.9300
C2—C1 1.353 (4) C23—C24 1.352 (6)
C2—H2 0.9300 C23—H23 0.9300
C8—C7 1.400 (5) C25—C24 1.381 (6)
C8—H8 0.9300 C25—H25 0.9300
C21—C26 1.376 (5) C24—H24 0.9300
C20—N1—C21 124.8 (3) C12—C13—H13 119.6
C20—N1—H55 122 (3) C7—C6—C5 121.0 (3)
C21—N1—H55 113 (3) C7—C6—H6 119.5
C4—C3—C2 123.6 (3) C5—C6—H6 119.5
C4—C3—C12 118.0 (2) C6—C7—C8 120.8 (3)
C2—C3—C12 118.4 (3) C6—C7—H7 119.6
C11—C12—C13 121.2 (3) C8—C7—H7 119.6
C11—C12—C3 120.6 (3) C17—C16—C15 121.5 (3)
C13—C12—C3 118.2 (3) C17—C16—H16 119.2
C10—C11—C12 120.1 (2) C15—C16—H16 119.2
C10—C11—C15 120.1 (2) C21—C26—C25 119.7 (4)
C12—C11—C15 119.8 (2) C21—C26—H26 120.2
C4—C5—C6 123.7 (3) C25—C26—H26 120.2
C4—C5—C10 118.1 (2) C17—C18—C19 120.2 (3)
C6—C5—C10 118.2 (3) C17—C18—H18 119.9
C11—C10—C9 121.9 (3) C19—C18—H18 119.9
C11—C10—C5 120.2 (2) C2—C1—C14 121.1 (3)
C9—C10—C5 118.0 (3) C2—C1—H1 119.5
C3—C4—C5 123.0 (3) C14—C1—H1 119.5
C3—C4—Br1 118.7 (2) C18—C19—C20 120.8 (3)
C5—C4—Br1 118.3 (2) C18—C19—H19 119.6
C20—C15—C16 118.6 (3) C20—C19—H19 119.6
C20—C15—C11 120.8 (3) C23—C22—C21 120.1 (3)
C16—C15—C11 120.6 (3) C23—C22—H22 119.9
C8—C9—C10 121.3 (3) C21—C22—H22 119.9
C8—C9—H9 119.4 C18—C17—C16 119.4 (3)
C10—C9—H9 119.4 C18—C17—H17 120.3
C15—C20—C19 119.4 (3) C16—C17—H17 120.3
C15—C20—N1 118.9 (3) C13—C14—C1 120.9 (3)
C19—C20—N1 121.7 (3) C13—C14—H14 119.5
C1—C2—C3 120.6 (3) C1—C14—H14 119.5
C1—C2—H2 119.7 C24—C23—C22 121.3 (4)
C3—C2—H2 119.7 C24—C23—H23 119.3
C9—C8—C7 120.7 (3) C22—C23—H23 119.3
C9—C8—H8 119.6 C24—C25—C26 120.7 (4)
C7—C8—H8 119.6 C24—C25—H25 119.7
C26—C21—C22 119.1 (3) C26—C25—H25 119.7
C26—C21—N1 119.3 (3) C23—C24—C25 119.1 (4)
C22—C21—N1 121.5 (3) C23—C24—H24 120.4
C14—C13—C12 120.8 (3) C25—C24—H24 120.4
C14—C13—H13 119.6
C4—C3—C12—C11 −0.2 (4) C11—C15—C20—N1 −2.8 (5)
C2—C3—C12—C11 178.7 (3) C21—N1—C20—C15 148.5 (3)
C4—C3—C12—C13 −179.9 (3) C21—N1—C20—C19 −32.9 (5)
C2—C3—C12—C13 −1.0 (4) C4—C3—C2—C1 178.5 (3)
C13—C12—C11—C10 178.9 (3) C12—C3—C2—C1 −0.3 (4)
C3—C12—C11—C10 −0.8 (4) C10—C9—C8—C7 −0.3 (5)
C13—C12—C11—C15 −1.1 (4) C20—N1—C21—C26 144.7 (4)
C3—C12—C11—C15 179.2 (2) C20—N1—C21—C22 −38.2 (5)
C12—C11—C10—C9 −179.0 (3) C11—C12—C13—C14 −178.4 (3)
C15—C11—C10—C9 1.0 (4) C3—C12—C13—C14 1.3 (5)
C12—C11—C10—C5 1.9 (4) C4—C5—C6—C7 −179.1 (3)
C15—C11—C10—C5 −178.1 (2) C10—C5—C6—C7 0.8 (4)
C4—C5—C10—C11 −2.0 (4) C5—C6—C7—C8 −0.2 (5)
C6—C5—C10—C11 178.1 (3) C9—C8—C7—C6 0.0 (5)
C4—C5—C10—C9 178.8 (2) C20—C15—C16—C17 1.9 (5)
C6—C5—C10—C9 −1.0 (4) C11—C15—C16—C17 −178.4 (3)
C2—C3—C4—C5 −178.8 (3) C22—C21—C26—C25 −0.4 (5)
C12—C3—C4—C5 0.0 (4) N1—C21—C26—C25 176.8 (3)
C2—C3—C4—Br1 1.3 (4) C3—C2—C1—C14 1.6 (5)
C12—C3—C4—Br1 −179.9 (2) C17—C18—C19—C20 1.0 (5)
C6—C5—C4—C3 −179.1 (3) C15—C20—C19—C18 0.4 (5)
C10—C5—C4—C3 1.1 (4) N1—C20—C19—C18 −178.3 (3)
C6—C5—C4—Br1 0.8 (4) C26—C21—C22—C23 −0.5 (5)
C10—C5—C4—Br1 −179.03 (19) N1—C21—C22—C23 −177.5 (3)
C10—C11—C15—C20 −86.9 (3) C19—C18—C17—C16 −0.9 (6)
C12—C11—C15—C20 93.1 (3) C15—C16—C17—C18 −0.5 (6)
C10—C11—C15—C16 93.3 (4) C12—C13—C14—C1 −0.1 (5)
C12—C11—C15—C16 −86.7 (4) C2—C1—C14—C13 −1.3 (5)
C11—C10—C9—C8 −178.3 (3) C21—C22—C23—C24 1.1 (6)
C5—C10—C9—C8 0.8 (4) C21—C26—C25—C24 0.6 (6)
C16—C15—C20—C19 −1.8 (5) C22—C23—C24—C25 −0.9 (6)
C11—C15—C20—C19 178.5 (3) C26—C25—C24—C23 0.0 (6)
C16—C15—C20—N1 176.9 (3)