| Agilent Xcalibur, Atlas, Gemini diffractometer | 3115 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.037 |
| ω scans | θmax = 26.4°, θmin = 3.4° |
| Absorption correction: analytical (CrysAlis RED; Agilent, 2012) | h = −16→14 |
| Tmin = 0.432, Tmax = 0.572 | k = −9→8 |
| 12046 measured reflections | l = −25→25 |
| 3999 independent reflections |
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