Table 3.

Validation parameters including coefficient of determination, LOD, LOQ, and matrix effect.

Carbamate	R2	Linear dynamic range (μg kg−1)	LOD (μg kg−1)	LOQ (μg kg−1)	Matrix effect (%)
Carbosulfan	0.9999	0.01–500	0.0107	0.0323	− 4.46
Phenmedipham	0.9998	0.001–100	0.0015	0.0044	10.92
Carbaryl	0.9997	0.001–100	0.0014	0.0043	− 4.98
Propoxur	0.9998	0.001–500	0.0011	0.0034	− 3.29
Propamocarb	0.9999	0.005–500	0.0049	0.0149	13.26
Aminocarb	0.9999	0.001–500	0.0010	0.0031	1.77
Ethiofencarb	0.9999	0.001–500	0.0011	0.0033	4.40
Pirimicarb	0.9999	0.005–100	0.0053	0.0162	0.71
Bendiocarb	0.9995	0.001–100	0.0014	0.0043	− 0.96
Fenoxycarb	0.9998	0.001–500	0.0011	0.0033	5.95
Carbofuran	0.9998	0.001–500	0.0011	0.0035	1.80
Methomyl	0.9998	0.01–500	0.0131	0.0398	4.82
Desmedipham	0.9998	0.001–500	0.0014	0.0043	0.71
Methiocarb	0.9999	0.001–500	0.0013	0.0041	0.28