Table 3. Yields of the Mo(IV) Nitrido Complex after Electrochemical Reduction of 1H with 1 Equiv DBU in THF under N₂.

no.	Eappl vs Fc+|0	number of e–	quantified by	yield (%)
1	–2.69 V	4	31P NMR	7
2	–2.82 V	2	31P NMR	0
3	–2.82 V	3	31P NMR	12
4	–2.93 V	3	NH3 release	14
5	–2.82 V	4	31P NMR	4
6	–3.08 V	5	31P NMR	18
7	–3.15 V	3	31P NMR	31a

^aBoron-doped diamond electrode instead of GC.