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. 2024 Jun 11;14(26):18608–18616. doi: 10.1039/d4ra01954g

13C (125 MHz) NMR data for compounds 1–4 in CDCl3 (δ in ppm).

No. 1 2 3 4
1 108.9, C 109.7, C 171.6, C 173.1, C
2 94.4, C 81.0, C 66.1, C 66.3, C
3 75.7, CH 81.3, CH 76.4, CH 76.4, CH
4 39.9, C 38.7, C 44.6, C 45.7, C
5 39.4, CH 39.6, CH 47.2, CH 51.8, CH
6 32.1, CH2 32.3CH2 32.3, CH2 72.1, CH
7 174.1, C 174.3, C 172.6, C 170.2, C
8 81.4, C 82.6, C 94.0, C 92.0, C
9 58.0, CH 58.5, CH 55.8, CH 55.2, CH
10 47.6, C 44.9, C 51.1, C 50.5, C
11 69.0, CH 69.2, CH 69.0, CH 21.8, CH2
12 36.2, CH2 36.0, CH2 34.0, CH2 34.2, CH2
13 41.8, C 41.8, C 41.2, C 35.3, C
14 71.3, C 71.3, C 71.3, C 42.4, CH
15 37.0, CH2 36.9, CH2 37.0, CH2 28.2, CH2
16 169.0, C 170.1, C 168.0, C 169.3, C
17 77.8, CH 78.0, CH 77.8, CH 77.8, CH
18 15.4, CH3 15.7, CH3 15.9, CH3 22.5, CH3
19 22.8, CH3 21.8, CH3 22.8, CH3 22.7, CH3
20 120.4, C 120.5, C 120.2, C 121.1, C
21 141.7, CH 141.6, CH 141.5, CH 140.6, CH
22 110.2, CH 110.2, CH 109.8, CH 109.5, CH
23 143.0, CH 142.8, CH 143.3, CH 143.6, CH
28 22.5, CH3 22.5, CH3 26.7, CH3 27.5, CH3
29 24.5, CH3 24.4, CH3 27.3, CH3 27.9, CH3
30 41.1, CH2 41.9, CH2 41.7, CH2 40.0, CH2
2-OAc 175.3, C
22.3, CH3
3-OAc 170.6, C 171.5, C 170.1, C 170.1, C
21.10, CH3 21.12, CH3 20.9, CH3 20.9, CH3
6-OAc 170.3, C
21.0, CH3
7-OCH3 52.2, CH3 52.1, CH3 52.1, CH3 52.9, CH3
11-OAc 169.8, C 169.8, C 169.8, C
21.08, CH3 21.07, CH3 21.2, CH3