Scheme 15.
Final steps in the total synthesis of RvD2n-3 DPA (20) using the Näf reduction protocol. Reagents and conditions: (i) Zn/KCN, 1-propanol/H2O, then TMSCHN2, toluene/MeOH; (ii) LiOH (aq), THF, −78 to 4 °C.
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