| Oxford Diffraction Xcalibur, Eos diffractometer | 2268 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 1793 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.041 |
| Detector resolution: 16.1419 pixels mm-1 | θmax = 30.9°, θmin = 2.8° |
| ω scan | h = −23→23 |
| Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2014) | k = −8→9 |
| Tmin = 0.275, Tmax = 1.000 | l = −22→23 |
| 19772 measured reflections |
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