Table 2.
Data collection | Glucose isomerase | Lysozyme |
---|---|---|
X-ray Source | 1C, PLS-II | 1C, PLS-II |
X-ray energy (eV) | 14820 | 14820 |
X-ray exposure (ms) | 100 | 100 |
Collected images | 20,210 | 18,959 |
Hit images | 13,592 | 9535 |
Indexed patterns | 17,626 | 3485 |
Space group | I222 | P43212 |
Cell dimension (Å) a, b, c |
94.14, 99.94, 103.16 |
78.83, 78.83, 38.20 |
Resolution (Å) | 20.00–1.70 (1.76–1.70) | 20.00–2.20 (2.27–2.20) |
Unique reflections | 53,508 (5307) | 6509 (628) |
Completeness (%) | 100.0 (100.0) | 100.0 (100.0) |
Redundancy | 191.5 (256.9) | 488.7 (398.5) |
SNR | 4.67 (4.39) | 5.43 (3.74) |
CC | 0.8239 (0.3692) | 0.8737 (0.5245) |
CC* | 0.9505 (0.7343) | 0.9657 (0.8295) |
Rsplit (%) a | 25.98 (27.16) | 21.21 (33.46) |
Wilson B factor (Å2) | 11.97 | 23.92 |
Values for the outer shell are given in parentheses.
Rsplit = , bRwork = Σ||Fobs|-|Fcalc||/Σ|Fobs|, where Fobs and Fcalc are the observed and calculated structure-factor amplitudes respectively.