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. 2024 Jul 10;87(7):1786–1797. doi: 10.1021/acs.jnatprod.4c00338

Figure 3.

Figure 3

Ketalization and Mosher esterification for compounds 5 and 6. ΔδS–R values for Mosher esters (5b/5c and 6b/6c) are shown. Reagents and conditions: (i) Acetone, p-toluene sulfonic acid (PDSA), 37 °C, 2 h; (ii) DMAP, (S)- or (R)-MTPA chloride, room temperature, 2 h.