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. 2024 Jul 10;87(7):1786–1797. doi: 10.1021/acs.jnatprod.4c00338

Table 1. 13C NMR (150 MHz) Data of 1–11 (CDCl3).

no. 1 2 3 4 5 6 7 8 9 10 11
1 34.7, CH 34.7, CH 34.6, CH 34.7, CH 34.8, CH 34.8, CH 34.8, CH 34.8, CH 34.7, CH 34.8, CH 34.8, CH
2 25.0, CH2 25.0, CH2 25.0, CH2 24.9, CH2 25.0, CH2 25.0, CH2 25.0, CH2 25.0, CH2 25.0, CH2 25.0, CH2 25.0, CH2
3 35.9, CH2 35.9, CH2 35.9, CH2 35.9, CH2 36.0, CH2 36.0, CH2 36.0, CH2 36.0, CH2 36.0, CH2 36.0, CH2 36.0, CH2
4 70.6, CH 70.6, CH 71.5, CH 71.2, CH 70.5, CH 70.5, CH 70.4, CH 70.5, CH 71.2, CH 70.5, CH 70.4, CH
5 22.9, CH 22.9, CH 22.9, CH 22.9, CH 22.9, CH2 22.9, CH 22.9, CH 22.9, CH 22.9, CH 22.9, CH 22.9, CH2
6 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2 30.8, CH2
7 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH 37.8, CH
8 75.8, CH 75.8, CH 75.6, CH 75.7, CH 75.7, CH 75.7, CH 75.7, CH 75.7, CH 75.6, CH 75.7, CH 75.7, CH
9 37.4, CH2 37.4, CH2 37.3, CH2 37.3, CH2 37.4, CH2 37.4, CH2 37.4, CH2 37.4, CH2 37.4, CH2 37.4, CH2 37.4, CH2
10 17.1, C 17.1, C 17.1, C 17.0, C 17.1, C 17.1, C 17.1, C 17.1, C 17.1, C 17.1, C 17.1, C
11 139.0, C 139.0, C 139.0, C 139.1, C 139.0, C 139.0, C 139.0, C 139.0, C 139.0, C 139.0, C 139.0, C
12 170.6, C 170.7, C 170.5, C 170.7, C 170.6, C 170.6, C 170.6, C 170.6, C 170.5, C 170.6, C 170.5, C
13 122.7, CH2 122.7, CH2 122.6, CH2 122.6, CH2 122.6, CH2 122.6, CH2 122.6, CH2 122.6, CH2 122.6, CH2 122.6, CH2 122.5, CH2
14 18.3, CH3 18.3, CH3 18.3, CH3 18.2, CH3 18.3, CH3 18.3, CH3 18.3, CH3 18.3, CH3 18.3, CH3 18.2, CH3 18.2, CH3
15 20.0, CH3 20.0, CH3 20.0, CH3 20.0, CH3 20.0, CH3 20.0, CH3 20.0, CH3 20.0, CH3 19.9, CH3 20.0, CH3 20.0, CH3
1′ 173.5, C 173.5, C 171.5, C 171.4, C 173.5, C 173.5, C 173.5, C 173.5, C 172.7, C 173.5, C 173.5, C
2′ 34.6, CH2 34.6, CH2 36.5, CH2 38.8, CH2 34.7, CH2 34.7, CH2 34.7, CH2 34.7, CH2 41.6, CH2 34.7, CH2 34.7, CH2
3′ 24.9, CH2 24.9a, CH2 36.4, CH 125.3, C 25.1a, CH2 25.0a, CH2 25.1, CH2 25.0, CH2 68.1, CH 25.0, CH2 25.1, CH2
4′ 29.2b, CH2 28.9b, CH2 163.1, C 138.4, C 25.1a, CH2 25.1a, CH2 29.1b, CH2 29.2b, CH2 36.6, CH2 28.9b, CH2 29.5b, CH2
5′ 29.0b, CH2 29.0b, CH2 127.7, CH 117.2, CH 37.2, CH2 37.4, CH2 29.2b, CH2 29.1b, CH2 25.5, CH2 28.8b, CH2 29.3b, CH2
6′ 28.9b, CH2 28.9b, CH2 198.8, C 154.6, C 72.3, CH 72.1, CH 29.4b, CH2 29.2b, CH2 29.6b, CH2 28.9b, CH2 29.2b, CH2
7′ 25.4, CH2 25.1a, CH2 34.1, CH2 112.8, CH 136.5, CH 136.5, CH 29.5b, CH2 25.7, CH2 29.6b, CH2 24.7, CH2 29.b, CH2
8′ 28.3, CH2 33.1, CH2 27.4, CH2 131.3, CH 129.9, CH 129.5, CH 29.6b, CH2 32.7, CH2 29.7b, CH2 34.1, CH2 27.2a, CH2
9′ 84.7, CH 87.5, CH 22.7, CH3 19.7, CH3 75.5, CH 75.6, CH 37.5, CH2 63.0, CH2 29.7b, CH2 179.0, C 130.0, CH
10′ 69.0, CH 71.8, CH     74.5, CH 74.6, CH 72.0, CH   29.7b, CH2   129.7, CH
11′ 39.4, CH2 37.7, CH2     32.9, CH2 32.9, CH2 37.4, CH2   29.7b, CH2   27.1a, CH2
12′ 175.4, C 174.8, C     25.0a, CH2 25.0a, CH2 25.7a, CH2   29.6b, CH2   29.7b, CH2
13′         29.0b, CH2 29.0b, CH2 25.6a, CH2   29.4b, CH2   29.1b, CH2
14′         29.2b, CH2 29.0b, CH2 25.6a, CH2   29.7b, CH2   29.1b, CH2
15′         29.4b, CH2 29.4b, CH2 32.7, CH2   31.9, CH2   29.1b, CH2
16′         31.7, CH2 31.7, CH2 63.0, CH3   22.7, CH2   31.9, CH2
17′         22.6, CH2 22.6, CH2     14.1, CH3   22.7, CH2
18′         14.0, CH3 14.0, CH3         14.1, CH3
a,b

Assignments may be interchanged within the same column.