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. Author manuscript; available in PMC: 2024 Aug 2.
Published in final edited form as: Bioorg Chem. 2020 Mar 9;98:103744. doi: 10.1016/j.bioorg.2020.103744

Table 1.

13CNMR assignments for compounds 1 and 2a

Position 1 2 Position 1 2
1 38.75 22.29 16 26.32 36.65
2 27.10 41.53 17 32.65 30.13
3 79.19 213.21 18 47.40 44.26
4 38.94 58.29 19 47.00 29.40
5 55.34 42.07 20 31.24 40.44
6 18.54 41.37 21 34.90 30.29
7 32.82 18.26 22 37.31 35.33
8 41.89 50.75 23 28.56 6.81
9 47.80 37.47 24 15.65 14.67
10 37.12 59.83 25 15.74 18.42
11 23.85 36.18 26 16.97 16.35
12 121.89 29.57 27 26.15 18.11
13 145.35 39.26 28 27.40 31.84
14 39.96 39.20 29 33.49 184.12
15 28.26 29.50 30 23.69 31.53
a

13CNMR spectra were obtained at 100 MHz, and recorded in CDCl3 at room temperature.