Table 1. Experimental details.
| Crystal data | |
| Chemical formula | C12H8F2N2·C2H4O2 |
| M r | 278.26 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 100 |
| a, b, c (Å) | 3.8047 (1), 11.0101 (4), 15.4968 (6) |
| α, β, γ (°) | 79.535 (1), 89.223 (1), 82.880 (1) |
| V (Å3) | 633.42 (4) |
| Z | 2 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.12 |
| Crystal size (mm) | 0.35 × 0.28 × 0.21 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 11642, 2896, 2531 |
| R int | 0.083 |
| (sin θ/λ)max (Å−1) | 0.650 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.038, 0.110, 1.06 |
| No. of reflections | 2896 |
| No. of parameters | 185 |
| No. of restraints | 1 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.39, −0.28 |
