| Crystal data |
| Chemical formula |
[RhCl(C8H12)(C8H15N3)] |
|
M
r
|
399.76 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
9.6253 (1), 13.6771 (2), 13.7938 (2) |
| α, β, γ (°) |
76.410 (1), 83.455 (1), 80.345 (1) |
|
V (Å3) |
1734.78 (4) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
1.14 |
| Crystal size (mm) |
0.30 × 0.23 × 0.15 |
| |
| Data collection |
| Diffractometer |
Rigaku XtaLAB Synergy-S |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2024 ▸) |
|
Tmin, Tmax
|
0.770, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
52942, 8619, 7885 |
|
R
int
|
0.037 |
| (sin θ/λ)max (Å−1) |
0.667 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.025, 0.066, 1.03 |
| No. of reflections |
8619 |
| No. of parameters |
385 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.02, −0.50 |
