Table 2. Experimental details.
| Crystal data | |
| Chemical formula | (C2H10N2)2[(C10H12N2O8)(MoO3)2]·4H2O |
| M r | 772.40 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 150 |
| a, b, c (Å) | 22.5897 (14), 7.5100 (4), 16.3743 (10) |
| β (°) | 94.716 (2) |
| V (Å3) | 2768.5 (3) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.00 |
| Crystal size (mm) | 0.17 × 0.17 × 0.13 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| Tmin, Tmax | 0.691, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 24031, 3192, 2946 |
| R int | 0.032 |
| (sin θ/λ)max (Å−1) | 0.650 |
| Refinement | |
| R[F2 > 2σ(F2)], wR(F2), S | 0.022, 0.060, 1.06 |
| No. of reflections | 3192 |
| No. of parameters | 189 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.67, −1.06 |