| Crystal data |
| Chemical formula |
[PdCl2(C22H21NO)2] |
|
M
r
|
808.09 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
10.2505 (4), 18.6165 (9), 10.6345 (5) |
| β (°) |
96.388 (4) |
|
V (Å3) |
2016.77 (16) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.63 |
| Crystal size (mm) |
0.27 × 0.15 × 0.09 |
| |
| Data collection |
| Diffractometer |
Xcalibur, Atlas, Gemini |
| Absorption correction |
Analytical CrysAlis PRO (Agilent, 2013 ▸) |
|
Tmin, Tmax
|
0.938, 0.976 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
25419, 10009, 6673 |
|
R
int
|
0.040 |
| (sin θ/λ)max (Å−1) |
0.706 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.041, 0.077, 1.02 |
| No. of reflections |
10009 |
| No. of parameters |
464 |
| No. of restraints |
108 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.53, −0.30 |
| Absolute structure |
Flack x determined using 2435 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.00 (3) |
