. 2024 Jul 26;146(31):21889–21902. doi: 10.1021/jacs.4c06304

Table I. δ_iso (ppm), δ_csa (ppm), η_csa, Line Widths (ppm), and Relative Intensities^a.

	δ_iso	δ_csa	η_csa	LW	I	assignment
line 1	12.8	–159	0.65	17.1	32.0	Ti–F–Ti
line 2	20.0	–204	0.00	31.8	65.8	Ti–F–Ti
line 3	169.2	–113	0.00	80.6	2.2	Ti–F–□

Averaging over lines 1 and 2 gives a weighted average for bridging Ti–F–Ti environments ⟨δ_iso⟩ = 17.6 ppm.

Table I. δiso (ppm), δcsa (ppm), ηcsa, Line Widths (ppm), and Relative Intensitiesa.