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. 2000 Nov 1;28(21):4382–4390. doi: 10.1093/nar/28.21.4382

Table 1. Recovery in individual steps of synthesis, shown as molar percent.

  Recovery (%)
  Step Overall
2′-deoxyadenosine-5′-monophosphate 100 100
N1-(2-aminoethyl)-2′-deoxyadenosine-5′-monophosphate 50.9 50.9
N6-(2-aminoethyl)-2′-deoxyadenosine-5′-monophosphate 25.0 12.7
N6-[trifluoroacetyl-(2-aminoethyl)]-2′-deoxyadenosine-5′-monophosphate 63.7 8.1
N6-[trifluoroacetyl-(2-aminoethyl)]-2′-deoxyadenosine-5′-triphosphate 63.8 5.2
N6-(2-aminoethyl)-2′-deoxyadenosine-5′-triphosphate 69.4 3.6
N6-[4-azidobenzoyl-(2-aminoethyl)]-2′-deoxyadenosine-5′-triphosphate 56.2 2.0
N6-[4-[3-(trifluoromethyl)-diazirin-3-yl]benzoyl-(2-aminoethyl)]-2′-deoxyadenosine-5′-triphosphate 86.0 3.1