Table 2.
13C NMR spectroscopic data of silvaticusins A–C (1–3) (δ in ppm)
| No | 1a | 2a | 3b |
|---|---|---|---|
| 1 | 31.0, CH2 | 30.9, CH2 | 30.3, CH2 |
| 2 | 41.5, CH2 | 19.0, CH2 | 26.4, CH2 |
| 3 | 19.1, CH2 | 40.9, CH2 | 70.6, CH |
| 4 | 34.0, C | 34.0, C | 55.1, C |
| 5 | 57.8, CH | 48.9, CH | 43.6, CH |
| 6 | 73.3, CH | 32.3, CH2 | 30.9, CH2 |
| 7 | 99.9, C | 98.1, C | 72.6, CH |
| 8 | 53.5, C | 59.8, C | 60.8, C |
| 9 | 40.0, CH | 48.9, CH | 53.3, CH |
| 10 | 36.1, C | 36.1, C | 37.6, C |
| 11 | 27.1, CH2 | 28.2, CH2 | 17.0, CH2 |
| 12 | 76.5, CH | 74.7, CH | 36.8, CH2 |
| 13 | 57.9, CH | 55.3, CH | 45.8, CH |
| 14 | 74.3, CH | 71.9, CH | 74.5, CH |
| 15 | 73.3, CH | 203.3, C | 206.6, C |
| 16 | 156.3, C | 149.7, C | 148.5, C |
| 17 | 111.1, CH2 | 119.1, CH2 | 115.6, CH2 |
| 18 | 33.6, CH3 | 20.8, CH3 | 205.8, CH |
| 19 | 22.5, CH3 | 32.4, CH3 | 8.6, CH3 |
| 20 | 65.7, CH2 | 66.4, CH2 | 17.3, CH3 |
aRecorded on a 500 MHz NMR spectrometer in pyridine-d5. bRecorded on a 600 MHz NMR spectrometer in pyridine-d5