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A series of EXSY spectra with an 80 ms mixing time were collected from 298–348 K for 9, to calculate the rotamer rate of exchange. The exchange peaks between the syn and anti rotamers were integrated at each temperature (A) and the exchange rate was plotted (B). From the exchange rate, an Eyring plot was calculated (C) and both the torsion rotation and energy of rotation were determined for the compound.
