Table 2.
Operation | Temperature (°C) | Heating Rate (°C s−1) | Holding Time (s) | Argon Flow |
---|---|---|---|---|
Drying | 90 | 10 | 10 | Maximal |
Drying | 100 | 5 | 10 | Maximal |
Drying | 120 | 5 | 15 | Maximal |
Pyrolysis | 400 | 50 | 20 | Maximal |
Pyrolysis | 1900 | 500 | 10 | Maximal |
Auto-zero | 1900 | 0 | 5 | Stop |
Atomization | 2800 | 1500 | 5 | Stop |
Cleaning | 2850 | 500 | 5 | Maximal |