| Ni1—N11 | 2.1388 (19) | C25—H25 | 0.9500 |
| Ni1—N21 | 2.1544 (19) | C26—H26 | 0.9500 |
| Ni1—N31 | 2.1621 (18) | C27—H27A | 0.9800 |
| Ni1—N41 | 2.2056 (18) | C27—H27B | 0.9800 |
| Ni1—Cl1 | 2.3658 (6) | C27—H27C | 0.9800 |
| Ni1—Cl2 | 2.4051 (6) | N31—C31 | 1.440 (3) |
| N11—C11 | 1.428 (3) | N31—H31A | 0.91 (2) |
| N11—H11A | 0.85 (2) | N31—H31B | 0.85 (2) |
| N11—H11B | 0.83 (2) | C31—C36 | 1.381 (3) |
| C11—C16 | 1.385 (3) | C31—C32 | 1.391 (3) |
| C11—C12 | 1.392 (3) | C32—C33 | 1.388 (3) |
| C12—C13 | 1.384 (3) | C32—H32 | 0.9500 |
| C12—H12 | 0.9500 | C33—C34 | 1.388 (3) |
| O13—C13 | 1.367 (3) | C34—C35 | 1.379 (3) |
| O13—C17 | 1.428 (3) | C34—H34 | 0.9500 |
| C13—C14 | 1.387 (3) | C35—C36 | 1.388 (3) |
| C14—C15 | 1.382 (3) | C35—H35 | 0.9500 |
| C14—H14 | 0.9500 | C36—H36 | 0.9500 |
| C15—C16 | 1.390 (3) | C37—H37A | 0.9800 |
| C15—H15 | 0.9500 | C37—H37B | 0.9800 |
| C16—H16 | 0.9500 | C37—H37C | 0.9800 |
| C17—H17A | 0.9800 | N41—C41 | 1.436 (3) |
| C17—H17B | 0.9800 | N41—H41A | 0.81 (2) |
| C17—H17C | 0.9800 | N41—H41B | 0.83 (2) |
| N21—C21 | 1.430 (3) | C41—C42 | 1.381 (3) |
| N21—H21A | 0.86 (2) | C41—C46 | 1.390 (3) |
| N21—H21B | 0.85 (2) | C42—C43 | 1.387 (3) |
| C21—C26 | 1.379 (3) | C42—H42 | 0.9500 |
| C21—C22 | 1.393 (3) | O43—C43 | 1.370 (3) |
| O33—C33 | 1.368 (3) | O43—C47 | 1.428 (3) |
| O33—C37 | 1.431 (3) | C43—C44 | 1.385 (3) |
| C22—C23 | 1.391 (3) | C44—C45 | 1.383 (3) |
| C22—H22 | 0.9500 | C44—H44 | 0.9500 |
| O23—C23 | 1.366 (3) | C45—C46 | 1.380 (3) |
| O23—C27 | 1.430 (3) | C45—H45 | 0.9500 |
| C23—C24 | 1.391 (3) | C46—H46 | 0.9500 |
| C24—C25 | 1.371 (3) | C47—H47A | 0.9800 |
| C24—H24 | 0.9500 | C47—H47B | 0.9800 |
| C25—C26 | 1.397 (3) | C47—H47C | 0.9800 |
| N11—Ni1—N21 | 178.52 (8) | C21—C26—H26 | 120.6 |
| N11—Ni1—N31 | 94.62 (7) | C25—C26—H26 | 120.6 |
| N21—Ni1—N31 | 86.39 (7) | O23—C27—H27A | 109.5 |
| N11—Ni1—N41 | 84.25 (7) | O23—C27—H27B | 109.5 |
| N21—Ni1—N41 | 94.75 (7) | H27A—C27—H27B | 109.5 |
| N31—Ni1—N41 | 178.66 (8) | O23—C27—H27C | 109.5 |
| N11—Ni1—Cl1 | 90.80 (6) | H27A—C27—H27C | 109.5 |
| N21—Ni1—Cl1 | 88.04 (6) | H27B—C27—H27C | 109.5 |
| N31—Ni1—Cl1 | 94.66 (5) | C31—N31—Ni1 | 125.09 (14) |
| N41—Ni1—Cl1 | 86.07 (5) | C31—N31—H31A | 110.5 (15) |
| N11—Ni1—Cl2 | 89.10 (6) | Ni1—N31—H31A | 100.9 (14) |
| N21—Ni1—Cl2 | 92.06 (6) | C31—N31—H31B | 109.2 (16) |
| N31—Ni1—Cl2 | 85.45 (5) | Ni1—N31—H31B | 101.4 (16) |
| N41—Ni1—Cl2 | 93.82 (5) | H31A—N31—H31B | 109 (2) |
| Cl1—Ni1—Cl2 | 179.86 (2) | C36—C31—C32 | 120.8 (2) |
| C11—N11—Ni1 | 120.77 (14) | C36—C31—N31 | 120.7 (2) |
| C11—N11—H11A | 109.6 (16) | C32—C31—N31 | 118.46 (19) |
| Ni1—N11—H11A | 100.8 (16) | C33—C32—C31 | 119.3 (2) |
| C11—N11—H11B | 107.7 (16) | C33—C32—H32 | 120.3 |
| Ni1—N11—H11B | 106.1 (17) | C31—C32—H32 | 120.3 |
| H11A—N11—H11B | 112 (2) | O33—C33—C32 | 123.3 (2) |
| C16—C11—C12 | 120.4 (2) | O33—C33—C34 | 116.24 (19) |
| C16—C11—N11 | 121.1 (2) | C32—C33—C34 | 120.4 (2) |
| C12—C11—N11 | 118.4 (2) | C35—C34—C33 | 119.3 (2) |
| C13—C12—C11 | 119.5 (2) | C35—C34—H34 | 120.4 |
| C13—C12—H12 | 120.3 | C33—C34—H34 | 120.4 |
| C11—C12—H12 | 120.3 | C34—C35—C36 | 121.2 (2) |
| C13—O13—C17 | 116.54 (18) | C34—C35—H35 | 119.4 |
| O13—C13—C12 | 122.6 (2) | C36—C35—H35 | 119.4 |
| O13—C13—C14 | 116.7 (2) | C31—C36—C35 | 119.0 (2) |
| C12—C13—C14 | 120.7 (2) | C31—C36—H36 | 120.5 |
| C15—C14—C13 | 119.2 (2) | C35—C36—H36 | 120.5 |
| C15—C14—H14 | 120.4 | O33—C37—H37A | 109.5 |
| C13—C14—H14 | 120.4 | O33—C37—H37B | 109.5 |
| C14—C15—C16 | 121.0 (2) | H37A—C37—H37B | 109.5 |
| C14—C15—H15 | 119.5 | O33—C37—H37C | 109.5 |
| C16—C15—H15 | 119.5 | H37A—C37—H37C | 109.5 |
| C11—C16—C15 | 119.2 (2) | H37B—C37—H37C | 109.5 |
| C11—C16—H16 | 120.4 | C41—N41—Ni1 | 123.17 (14) |
| C15—C16—H16 | 120.4 | C41—N41—H41A | 109.1 (18) |
| O13—C17—H17A | 109.5 | Ni1—N41—H41A | 101.2 (17) |
| O13—C17—H17B | 109.5 | C41—N41—H41B | 109.4 (17) |
| H17A—C17—H17B | 109.5 | Ni1—N41—H41B | 104.0 (17) |
| O13—C17—H17C | 109.5 | H41A—N41—H41B | 109 (2) |
| H17A—C17—H17C | 109.5 | C42—C41—C46 | 120.3 (2) |
| H17B—C17—H17C | 109.5 | C42—C41—N41 | 120.1 (2) |
| C21—N21—Ni1 | 116.21 (14) | C46—C41—N41 | 119.6 (2) |
| C21—N21—H21A | 109.8 (15) | C41—C42—C43 | 119.9 (2) |
| Ni1—N21—H21A | 105.2 (16) | C41—C42—H42 | 120.1 |
| C21—N21—H21B | 107.8 (16) | C43—C42—H42 | 120.1 |
| Ni1—N21—H21B | 104.7 (16) | C43—O43—C47 | 116.84 (18) |
| H21A—N21—H21B | 113 (2) | O43—C43—C44 | 123.7 (2) |
| C26—C21—C22 | 120.7 (2) | O43—C43—C42 | 115.7 (2) |
| C26—C21—N21 | 120.4 (2) | C44—C43—C42 | 120.6 (2) |
| C22—C21—N21 | 118.6 (2) | C45—C44—C43 | 118.7 (2) |
| C33—O33—C37 | 116.88 (17) | C45—C44—H44 | 120.7 |
| C23—C22—C21 | 119.3 (2) | C43—C44—H44 | 120.7 |
| C23—C22—H22 | 120.4 | C46—C45—C44 | 121.7 (2) |
| C21—C22—H22 | 120.4 | C46—C45—H45 | 119.2 |
| C23—O23—C27 | 117.27 (17) | C44—C45—H45 | 119.2 |
| O23—C23—C24 | 115.8 (2) | C45—C46—C41 | 119.0 (2) |
| O23—C23—C22 | 123.7 (2) | C45—C46—H46 | 120.5 |
| C24—C23—C22 | 120.5 (2) | C41—C46—H46 | 120.5 |
| C25—C24—C23 | 119.1 (2) | O43—C47—H47A | 109.5 |
| C25—C24—H24 | 120.5 | O43—C47—H47B | 109.5 |
| C23—C24—H24 | 120.5 | H47A—C47—H47B | 109.5 |
| C24—C25—C26 | 121.6 (2) | O43—C47—H47C | 109.5 |
| C24—C25—H25 | 119.2 | H47A—C47—H47C | 109.5 |
| C26—C25—H25 | 119.2 | H47B—C47—H47C | 109.5 |
| C21—C26—C25 | 118.8 (2) | ||
| Ni1—N11—C11—C16 | 102.6 (2) | Ni1—N31—C31—C36 | 88.5 (2) |
| Ni1—N11—C11—C12 | −75.6 (2) | Ni1—N31—C31—C32 | −91.6 (2) |
| C16—C11—C12—C13 | 0.3 (3) | C36—C31—C32—C33 | −0.2 (3) |
| N11—C11—C12—C13 | 178.5 (2) | N31—C31—C32—C33 | 179.85 (19) |
| C17—O13—C13—C12 | −10.9 (3) | C37—O33—C33—C32 | −1.4 (3) |
| C17—O13—C13—C14 | 169.4 (2) | C37—O33—C33—C34 | 178.35 (19) |
| C11—C12—C13—O13 | 178.8 (2) | C31—C32—C33—O33 | −179.19 (19) |
| C11—C12—C13—C14 | −1.5 (3) | C31—C32—C33—C34 | 1.1 (3) |
| O13—C13—C14—C15 | −178.7 (2) | O33—C33—C34—C35 | 179.2 (2) |
| C12—C13—C14—C15 | 1.5 (4) | C32—C33—C34—C35 | −1.0 (3) |
| C13—C14—C15—C16 | −0.4 (4) | C33—C34—C35—C36 | 0.2 (3) |
| C12—C11—C16—C15 | 0.8 (3) | C32—C31—C36—C35 | −0.6 (3) |
| N11—C11—C16—C15 | −177.4 (2) | N31—C31—C36—C35 | 179.3 (2) |
| C14—C15—C16—C11 | −0.8 (4) | C34—C35—C36—C31 | 0.7 (3) |
| Ni1—N21—C21—C26 | 90.7 (2) | Ni1—N41—C41—C42 | −84.4 (2) |
| Ni1—N21—C21—C22 | −84.6 (2) | Ni1—N41—C41—C46 | 92.3 (2) |
| C26—C21—C22—C23 | −0.3 (3) | C46—C41—C42—C43 | −0.9 (3) |
| N21—C21—C22—C23 | 174.9 (2) | N41—C41—C42—C43 | 175.75 (19) |
| C27—O23—C23—C24 | 173.2 (2) | C47—O43—C43—C44 | −0.5 (3) |
| C27—O23—C23—C22 | −7.8 (3) | C47—O43—C43—C42 | 179.32 (19) |
| C21—C22—C23—O23 | −179.01 (19) | C41—C42—C43—O43 | 179.42 (19) |
| C21—C22—C23—C24 | 0.0 (3) | C41—C42—C43—C44 | −0.7 (3) |
| O23—C23—C24—C25 | 179.2 (2) | O43—C43—C44—C45 | −178.6 (2) |
| C22—C23—C24—C25 | 0.2 (4) | C42—C43—C44—C45 | 1.5 (3) |
| C23—C24—C25—C26 | 0.0 (4) | C43—C44—C45—C46 | −0.7 (4) |
| C22—C21—C26—C25 | 0.5 (3) | C44—C45—C46—C41 | −0.9 (4) |
| N21—C21—C26—C25 | −174.7 (2) | C42—C41—C46—C45 | 1.7 (3) |
| C24—C25—C26—C21 | −0.3 (4) | N41—C41—C46—C45 | −175.0 (2) |