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. 2024 Sep 5;14(39):28401–28414. doi: 10.1039/d4ra04344h

Structural parameters of the as-grown CTS crystals calculated from the XRD pattern.

2θ (Degree) Crystallite size (D) (nm) (hkl) d-spacing (Å)
Observed Calculated % error
28.43 28.59 0.55 7.94 (111) 3.13
32.95 33.13 0.54 8.03 (200) 2.71
47.29 47.56 0.56 8.40 (220) 1.92
56.10 56.43 0.58 8.72 (311) 1.63
69.08 69.53 0.64 9.35 (400) 1.35
76.42 76.84 0.54 9.80 (331) 1.24