Crystal structure of (1,4,7,10,13,16-hexa­oxa­cycloocta­decane-κ6O)potassium-μ-oxalato-tri­phenylstannate(IV), the first reported 18-crown-6-stabilized potassium salt of tri­phenyl­oxalatostannate

. 2024 Aug 13;80(Pt 9):951–955. doi: 10.1107/S2056989024007758

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Sn1	0.0258 (2)	0.01459 (18)	0.0242 (2)	0.0024 (3)	−0.00227 (13)	0.0011 (3)
O1	0.026 (3)	0.016 (2)	0.024 (3)	0.002 (2)	−0.0018 (19)	0.001 (2)
O2	0.045 (4)	0.016 (3)	0.043 (4)	−0.001 (3)	−0.018 (3)	−0.001 (3)
O3	0.061 (5)	0.022 (3)	0.053 (5)	−0.004 (3)	−0.024 (3)	−0.002 (3)
O4	0.034 (3)	0.025 (3)	0.031 (3)	−0.003 (2)	−0.007 (2)	−0.002 (2)
C1	0.027 (3)	0.021 (5)	0.027 (3)	0.014 (3)	−0.005 (3)	−0.001 (3)
C2	0.038 (5)	0.020 (4)	0.030 (5)	0.006 (3)	−0.007 (3)	−0.003 (3)
C3	0.036 (5)	0.034 (5)	0.043 (5)	0.023 (4)	−0.008 (4)	−0.012 (4)
C4	0.030 (4)	0.046 (8)	0.044 (5)	0.001 (4)	0.005 (3)	−0.022 (5)
C5	0.039 (5)	0.032 (5)	0.043 (6)	0.002 (4)	0.013 (4)	−0.010 (4)
C6	0.028 (4)	0.020 (4)	0.035 (5)	0.012 (3)	0.000 (3)	−0.003 (3)
C7	0.022 (4)	0.012 (3)	0.030 (5)	0.002 (3)	0.004 (3)	0.005 (3)
C8	0.024 (4)	0.023 (4)	0.024 (4)	0.006 (3)	0.005 (3)	0.001 (3)
C9	0.028 (4)	0.020 (3)	0.023 (4)	−0.001 (3)	0.006 (3)	−0.001 (3)
C10	0.032 (4)	0.008 (3)	0.027 (4)	0.002 (3)	0.000 (3)	0.002 (3)
C11	0.035 (4)	0.018 (3)	0.024 (4)	0.002 (3)	−0.008 (3)	0.002 (3)
C12	0.030 (4)	0.013 (4)	0.028 (5)	0.004 (3)	−0.003 (3)	0.002 (3)
C13	0.026 (3)	0.028 (4)	0.027 (3)	−0.005 (5)	−0.001 (2)	0.001 (5)
C14	0.038 (5)	0.022 (4)	0.023 (4)	−0.004 (3)	−0.001 (3)	0.004 (3)
C15	0.039 (5)	0.040 (5)	0.038 (5)	−0.010 (4)	0.012 (4)	−0.005 (4)
C16	0.039 (4)	0.034 (4)	0.032 (4)	−0.016 (6)	0.004 (3)	0.009 (6)
C17	0.038 (5)	0.041 (5)	0.030 (4)	−0.015 (4)	−0.006 (3)	0.017 (4)
C18	0.027 (4)	0.029 (4)	0.035 (5)	−0.008 (3)	0.001 (3)	0.000 (4)
C19	0.021 (4)	0.020 (4)	0.027 (4)	0.001 (3)	0.003 (3)	0.004 (3)
C20	0.032 (5)	0.020 (4)	0.029 (5)	−0.001 (3)	−0.010 (3)	0.004 (3)
K1	0.0241 (7)	0.0168 (7)	0.0240 (8)	−0.0005 (5)	0.0001 (5)	−0.0004 (5)
O5	0.026 (3)	0.017 (2)	0.026 (3)	0.000 (2)	0.0027 (19)	−0.0001 (19)
O6	0.022 (3)	0.020 (3)	0.032 (3)	−0.002 (2)	0.003 (2)	0.001 (2)
O7	0.033 (4)	0.026 (3)	0.023 (3)	0.003 (3)	0.002 (2)	0.001 (3)
O8	0.039 (3)	0.017 (3)	0.030 (3)	0.000 (2)	−0.002 (2)	−0.001 (2)
O9	0.026 (3)	0.026 (3)	0.037 (4)	0.004 (3)	0.007 (3)	0.003 (3)
O10	0.030 (3)	0.018 (3)	0.026 (3)	0.002 (2)	0.002 (2)	−0.002 (2)
C21	0.023 (4)	0.021 (4)	0.031 (4)	0.009 (3)	−0.004 (3)	−0.001 (3)
C22	0.027 (5)	0.032 (5)	0.029 (5)	0.000 (4)	0.006 (4)	−0.002 (4)
C23	0.039 (5)	0.028 (5)	0.042 (5)	−0.007 (4)	0.018 (4)	−0.001 (4)
C24	0.041 (5)	0.015 (4)	0.027 (4)	−0.006 (3)	0.007 (3)	−0.004 (3)
C25	0.048 (5)	0.031 (4)	0.025 (4)	−0.002 (4)	0.001 (4)	0.012 (4)
C26	0.045 (5)	0.018 (4)	0.035 (5)	0.003 (4)	−0.005 (4)	0.011 (3)
C27	0.047 (6)	0.029 (5)	0.040 (5)	0.014 (4)	−0.004 (4)	−0.002 (4)
C28	0.028 (4)	0.030 (4)	0.049 (6)	0.014 (4)	0.001 (4)	0.003 (4)
C29	0.029 (4)	0.025 (4)	0.054 (6)	0.000 (4)	0.011 (4)	−0.005 (4)
C30	0.041 (5)	0.031 (5)	0.025 (4)	0.005 (4)	0.013 (4)	−0.003 (4)
C31	0.032 (5)	0.019 (4)	0.027 (5)	−0.007 (3)	0.000 (4)	0.001 (3)
C32	0.028 (4)	0.026 (4)	0.020 (4)	−0.003 (3)	−0.002 (3)	0.003 (3)