| Crystal data |
| Chemical formula |
[KSn(C6H5)3(C2O4)(C12H24O6)] |
|
M
r
|
741.42 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
9.4060 (3), 19.3779 (4), 9.4225 (3) |
| β (°) |
97.925 (2) |
|
V (Å3) |
1701.02 (8) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.93 |
| Crystal size (mm) |
0.06 × 0.06 × 0.03 × 0.02 (radius) |
| |
| Data collection |
| Diffractometer |
Rigaku XtaLAB Synergy-S dual wavelength Mo/Cu |
| Absorption correction |
Multi-scan (CrysAlis PRO; Rigaku OD, 2022 ▸) |
|
Tmin, Tmax
|
0.913, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
15412, 7113, 6792 |
|
R
int
|
0.040 |
| (sin θ/λ)max (Å−1) |
0.649 |
| |
| Refinement |
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.033, 0.105, 1.08 |
| No. of reflections |
7113 |
| No. of parameters |
398 |
| No. of restraints |
1 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.28, −0.52 |
| Absolute structure |
Flack x determined using 2807 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
−0.08 (3) |
